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Australian Synchrotron Visit

AIG Victorian Branch Visit to the Australian Synchrotron

We were a happy team of geos that ventured beyond the MCG on the Monday after the AFL Grand Final in September to visit the Australian Synchrotron, which is about the size of the MCG!

Earlier this year Kaylene Camuti met the Synchrotron’s Dr Tamsyn Ross, who suggested that a group from the AIG should visit the facility. Consequently, a party of 17 from the Victorian branch made the trip to the Melbourne suburb of Clayton, near Monash University. We were greeted by Tamsyn and her colleagues, Dr Helen Brand, Dr Kathryn Spiers and Dr David Cookson, each of whom gave us a talk, and then guided our group around this most impressive facility. Images can be seen on Dropbox folder \AIG_Vic\Aus Synchrotron_2014-09-29.

It was a terrific visit. The Synchrotron is potentially a very powerful tool. We left the facility rather like a character in the Arthur C Clarke/Stanley Kubrick book/movie, 2001- A Space Odyssey – we’ve got ourselves this tool, but we’re not too sure where it’s going to lead us! But we are exploration geos so we’ve got to give it a go. David Cookson, who is Head of Beamline Science and Operations, was particularly keen to encourage smaller enterprises to use the Synchrotron, and emphasised that they would try to accommodate any testing that geologists might wish to do—at a modest rate. Note that for geos in New South Wales there is already a state-funded support scheme in place (see section on NSW Industry Synchrotron Access Scheme, below). It is also possible for geologists working in academia to apply for access through the merit system.

A synchrotron is a machine that produces intense light, which can be used to investigate the details of matter from the atomic- to the nano-scale.  It can be used for many different applications including, for example, determining mineral phases, characterising pore structures, or mapping mineral traces in sectioned rocks. The AS is currently used by scientists from a diverse range of disciplines including agriculture, pharmaceuticals, forensics, advanced materials – geologists and metallurgists already use it to study rocks and minerals, and there are many possibilities for professionals working in these fields.

The Australian Synchrotron

The Australian Synchrotron

In basic terms the Synchrotron comprises a centrally-located electron gun, an accelerator, an inner booster ring, and an outer storage ring. Electrons are generated by the electron gun and accelerated to near the speed of light before being transferred to the storage ring where they are manipulated to give off light. The electrons circulating the storage ring are kept at a constant energy, apparently completing 1.4 million laps of the storage ring every second for about three days, all the while being used to produce beams of intense synchrotron light. Radiating tangentially from the storage ring are nine ‘beamlines’ – where the light generated in the storage ring is conditioned (filtered and focussed) as it propagates.

Australian_Synchrotron

The Australian Synchrotron

1. Electron Gun: Electrons are generated inside an electron gun by heating a barium compound cathode to ~ 1000°C. Bunches of electrons are accelerated away from the cathode surface and out of the gun using 90,000 volts.

2. Linear Accelerator (Linac): In the Linac, the electrons are accelerated to 99.9987% of the speed of light. They exit the linear accelerator with 100MeV of energy. The energy used to accelerate the electrons comes from a radio frequency (RF) current of 3GHz. Radio frequencies are part of the electromagnetic spectrum, just like infrared light, but they have lower energy levels and therefore longer wavelengths. The spacing of the electron bunches matches the wavelength of the RF current, thus ensuring that the electrons receive a ‘push’ through the regions where the RF current is applied.

3. Booster Ring (synchrotron): The electrons are transferred from the Linac to the Booster Ring, where their energy is boosted to 3GeV using more RF energy. In the Booster Ring, dipole electromagnets force the electrons to adopt an almost circular path. The electrons complete approximately 1 million laps in half a second, before passing into the Storage Ring.

4. Storage Ring: In the Storage Ring, electrons circulate at aconstant energy for many hours, and continuously generate intense synchrotron light. To ensure the number of electrons circulating remains nearly constant, they can be topped up by injecting more into the ring approximately every few minutes. An electron will complete around 1.4 million laps of the Storage Ring every second.

5. Beamlines: The synchrotron light – created by bending the path of the electrons through magnetic fields – is then channelled from the Storage Ring down long pipelines, called beamlines, so that scientists can utilise it for research. Each beam line includes different types of filters, mirrors and other optical components that prepare the light for use in a range of different scientific experiments.

6. End Station: At the end of each beamline is an End Station – a laboratory where the synchrotron light interacts with a sample. Detectors positioned around the sample measure how the light is transmitted, emitted, scattered or diffracted (depending on the experiment) by the sample. Researchers use this information to determine the composition or atomic structure of the sample, or to create a map-like image of the sample.

From left to right:Tamsin Ross, Helen Brand and Kathryn Spiers who helped conduct the AIG tour of the Australian Synchrotron facility

From left to right:Tamsin Ross, Helen Brand and Kathryn Spiers who helped conduct the AIG tour of the Australian Synchrotron facility

 

For scientists visiting the Synchrotron the fun begins at the end of each beamline where the end-station and user cabin are located. Scientists mount samples in the end-station and control the experiment while sitting in the cabin. It is in the end-station that a geologist could present a sample to be zapped by the very narrow, very intense beam of light (at X-ray or infrared frequencies). Depending on the technique, a variety of detectors will measure how the light is transmitted, emitted, scattered or diffracted by the sample. On the XFM beamline a geologist could, for example, create an elemental map of the surface of a rock or mineral sample – but each of the nine beamlines has a unique function with a wealth of possibilities.

The XFM beamline at the Australian Synchrotron

The XFM beam line at the Australian Synchrotron

The primary capabilities and basic applications of each of the Synchrotron’s beamlines is given in the table below.  Uses of any given beamline may extend beyond what is given here, and interested parties are encouraged to enquire at the Synchrotron about any ideas they might have. Tamsyn Ross and her colleagues are preparing a technical article for AIG NEWS (Ross, T., et al, (in prep): working title is ‘Geological and metallurgical uses for the Australian Synchrotron’).

Australian Synchrotron Beamlines

Beamline

Description

IMBL
(Imaging and Medical Beamline
A beamline utilising higher energy X-rays that can be used for 3D    X-ray imaging with micron resolution – can be used to visualise the internal structure of samples non-destructively
IR Microscope
(Infrared Microscope)
An FTIR (Fourier transform infrared) system which mixes mid-infrared spectroscopy with fine resolution to give spatial mapping of organic compounds
FarIR/THz
(Far-Infrared/Terahertz Beamline)
An FTIR system which uses far-infrared spectroscopy to study molecular structure – often in gas phases

MX
(Macromolecular Crystallography)

A powerful facility for determining the arrangement of atoms and molecules in single crystals, providing detailed information on molecules ten to tens of thousands of atoms in size”A powerful facility for determining the arrangement of atoms and molecules in single crystals, providing detailed information on of molecules ten to tens of thousands of atoms in size
PD
(Powder Diffraction)
A facility for investigating the bulk properties of crystalline samples at high resolution – particularly useful for identifying and quantifying crystalline phases, as well as monitoring the behaviour of crystalline materials in non-ambient and dynamic environments
SAXS/WAXS
(Small Angle X-ray Scattering/Wide Angle X-ray Scattering)
A flexible beamline used for investigating features ranging in size from 1 to 100 nanometres in bulk solid or liquid samples – useful for determining particle and pore sizes in natural and man-made materials
Soft X-ray A beamline most suited to non-destructively characterising surfaces and near-surface interfacial layers
XAS
(X-ray Absorption Spectroscopy)
A beamline used particularly for investigating the oxidation state and coordination environment of atoms in solid and liquid samples
XFM
(X-ray Fluorescence Microscopy)
A powerful beamline regularly used for high-resolution elemental mapping of solid samples containing heavy elements

 

The Australian Synchrotron website also has a little information on each of the beamlines as PDF fact sheets which are available from the synchrotron website.

A rendered example of one of the Synchrotron’s beamlines being used for crystallography. Image courtesy of the Australian Synchrotron

ilmenite

Synchrotron image showing distribution of titanium (blue), niobium (green) and thorium (red) in ilmenite. Ilmenite sample courtesy of Peter Kappen, La Trope University; image from XFM beamline and CSIRO collaborators Chris Ryan, Robin Kirkham and Gareth Moorehead (no scale provided).

As mentioned above, for researchers working in industry in New South Wales there is a state-funded support scheme already in place.

NSW Industry Synchrotron Access Scheme

The NSW Industry Synchrotron Access Scheme is a program that is currently being run by the NSW government which allows bodies conducting commercially-relevant research within NSW to apply for fully-funded beamtime on any of the beamlines at the Australian Synchrotron. The advantages of applying for beamtime through the NSW Industry Synchrotron Access Scheme are that there is no need to publish the work (as would be necessary through the standard merit access program), little is required in the way of preparing a proposal for the work (with assistance from the applicant, the Synchrotron handles most of the paperwork) and access to the Synchrotron through this scheme is typically more rapid than through the merit access program (access to some beamlines may still be possible in late 2014). A further important point is that the applicant retains their IP on work.

The Beamline Industry Group is a group of scientists dedicated to supporting commercial research taking place at the Synchrotron, in particular that of applicants to the NSW Industry Synchrotron Access Scheme. They offer obligation-free exploratory talks about potential projects, assistance with experimental design and expert support during beamtime – other services available include data analysis and reporting.

Beamline Industry Group Homepage:   www.synchrotron.org.au

NSW Industry Access Page:  industry.synchrotron.org.au/industry-access/nsw

Geoff Hodgson
AIG Victoria Branch

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